HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 59536621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Methyl-6-methoxypyridine-3-boronic acid | HCID 2763084 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59536621 | HCID 59536621 | 62.3% |
Reaction Steps
Add hydrogen peroxide (7.69 mL, 89.8 mmol) to a stirred mixture of 2-methoxy-6-methyl-5-pyridylboronic acid (5.0 g, 30 mmol) in dichloromethane (100 mL) kept under nitrogen at room temperature. Stir overnight at ambient temperature, add water and extract the mixture with dichloromethane. Combine the organic phases, dry (MgSO4), filter and concentrate to afford 2.6 g (62%) of the title compound. MS (m/z)=140 [M+1]
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173821B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-15719b56bbb1479dae037ccbf7d0d6db |
| Source note | uspto-grants-2012_05 |