HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1922208Generated: November 2, 2026
HCID 20033363, compound → HCID 24821999, compound
https://huagongshe.com/reaction/1922208
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 20033363 | HCID 20033363 | — |
| Reactant | N-methyl-4-(2-(methylsulfinyl)benzo[d]oxazol-6-yloxy)picolinamide | HCID 57725414 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 24821999 | HCID 24821999 | — |
Reaction Steps
The 4-(2-methanesulfinyl-benzooxazol-6-yloxy)-pyridine-2-carboxylic acid methylamide from step 3 of Example 2 and 3-(2-piperidin-1-yl-ethyl)-phenylamine were dissolved in DMAC and heated in a CEM microwave reactor at 120° C. for 10 to 20 minutes. The crude reaction mixture was purified by preparatory reverse phase HPLC. MH+=472.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08173689B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-f9c61ba1629f4c6894b04da3655be9bc |
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| Source note | uspto-grants-2012_05 |
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