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HRID1922901

反应详情

EQUATION

反应方程式

HRID 1922901 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(c2coc3ccccc23)OC1(C)C
HCID43811031

3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1-benzofuran

C14H17BO3

结构：Cn1c(CN2CCC(C(C)(C)O)CC2)nc2c(N3CCOCC3)nc(Cl)nc21
HCID59603426

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(CN2CCC(C(C)(C)O)CC2)nc2c(N3CCOCC3)nc(-c3coc4ccccc34)nc21
HCID59605339

未命名化合物

PROCEDURE

实验过程

Following the procedures for 140, 2-(1-((2-chloro-9-methyl-6-morpholino-9H-purin-8-yl)methyl)piperidin-4-yl)propan-2-ol and 2-(benzofuran-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane was converted to 138. LCMS: M+H+=491.2. 1H-NMR (400 MHz, DMSO-d6): δ 8.75 (s, 1H), 8.58 (m, 1H), 7.66 (m, 1H), 7.40 (m, 2H), 4.66 (s, 2H), 4.31 (m, 4H), 3.90 (s, 3H), 3.80 (m, 4H), 3.68 (s, br, 1H), 3.12 (m, 2H), 2.90 (m, 2H), 1.90 (m, 2H), 1.56 (m, 3H), 1.06 (s, 6H)