HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzimidazole → HCID 59605781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzimidazole | HCID 11984 | — |
| Reactant | HCID 86648264 | HCID 86648264 | — |
| Product | HCID 59605781 | HCID 59605781 | — |
Reaction Steps
Following General Procedure I for Buchwald coupling, 2-methylbenzimidazole and 9-((2-chloro-9-methyl-6-morpholino-9H-purin-8-yl)methyl)-1,5-dioxa-9-azaspiro[5.5]undecane were reacted to give 400. LCMS m/z: 519.2 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08173650B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-4b0a969058114d84beedf060abba65b5 |
| Source note | uspto-grants-2012_05 |