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HRID1923256

反应详情

EQUATION

反应方程式

HRID 1923256 的结构方程式

REACTANTS

反应物

2
结构：CC(Br)C(N)=O
HCID101118

2-Bromopropanamide

C3H6BrNO

结构：Cc1nc2ccccc2n1-c1nc(N2CCOCC2)c2nc(CC3CCNCC3)n(C)c2n1
HCID59605636

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nc2ccccc2n1-c1nc(N2CCOCC2)c2nc(CC3CCN([C@@H](C)C(N)=O)CC3)n(C)c2n1
HCID59605640

未命名化合物

PROCEDURE

实验过程

Following General Procedure C, 4-(9-methyl-2-(2-methyl-1H-benzo[d]imidazol-1-yl)-8-(piperidin-4-ylmethyl)-9H-purin-6-yl)morpholine and 2-bromopropionamide were reacted to give the racemic mixture. The enantiomers were separated by SFC to give 560. LCMS m/z: 259.7 (2M+H+)

WORKUP

后处理

  1. customwere reacted
  2. customto give the racemic mixture
  3. customThe enantiomers were separated by SFC