HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → Carbonic acid, 2,2-difluoroethyl ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 15985040 | HCID 15985040 | — |
| Product | Carbonic acid, 2,2-difluoroethyl ethyl ester | HCID 15985039 | — |
Reaction Steps
2,2-Difluoroethyl ethyl carbonate was prepared as in [Synthesis of 2,2-Difluoroethyl Methyl Carbonate] of Example IV-1, except that ethyl chlorocarbonate (7.9 g, 0.073 mol) was substituted for methyl chlorocarbonate (6.9 g, 0.073 mol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178246B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-526099c6cf1c48cbad587ae9d30978cf |
| Source note | uspto-grants-2012_05 |