5-Hexenoic Acid → 82096-18-2
Reaction equation
[Br:1][CH2:2][C:3](=[O:10])[C:4](C)(C)[CH2:5][CH:6]=[CH2:7].[C:11](O)(=O)CCCC=C>>[Br:1][CH2:2][C:3](=[O:10])[CH2:4][CH2:5][CH2:6][CH:7]=[CH2:11]Participants
3
Procedure
The title compound was prepared according to the procedure described for Intermediate 4, using 5-hexenoic acid in place of 2,2-dimethylpent-4-enoic acid. 1H NMR (300 MHz, CDCl3) δ 5.77 (m, 1H), 5.05-4.98 (m, 2H), 3.87 (s, 2H), 2.66 (t, J 7.3, 2H), 2.89 (m, 2H), 2.09 (m, 2H).
Sources & evidence
- ORD record
- ord-19173bd3b080433e9e83b6822c353ae9
- Source dataset
- uspto-grants-2012_05
- Patent number
- US08178520B2
Reaction notes
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