HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → 1-(2,3-Dihydro-1,4-benzodioxin-5-yl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2',3'-Dihydroxyacetophenone | HCID 6429110 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(2,3-Dihydro-1,4-benzodioxin-5-yl)ethanone | HCID 21268052 | — |
Reaction Steps
Prepared by reacting 1-(2,3-dihydroxy-phenyl)-ethanone with 1,2-dibromoethane in the presence of potassium carbonate in N,N-dimethylformamide at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178541B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-c8eda36796db4a7a9144527e1f4fe082 |
| Source note | uspto-grants-2012_05 |