Phenylhydrazine → HCID 46219578, 화합물

HRID 1924505노트

반응식

HRID 1924505 반응식
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([O:20][C:21]([F:24])([F:23])[F:22])[CH:15]=2)[N:8]=1)=O.[C:26]1([NH:32]N)[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[C:26]1([N:32]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[C:16]([O:20][C:21]([F:24])([F:23])[F:22])[CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1

참가 물질

3

반응물 2

HCID 7516PhenylhydrazineHCID 593701233-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

생성물 1

HCID 46219578HCID 46219578, 화합물수율 64%

실험 절차

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-6) and phenylhydrazine according to the method described for Example 1 in 64% yield. MS: M=399.1 (M+H)+

후처리

  1. customThe product was obtained

출처 및 근거

ORD 기록
ord-07447e052e1a40e88a3721e2b73e88f1
출처 데이터셋
uspto-grants-2012_05
특허 번호
US08178538B2

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