(4-Methylphenyl)hydrazine → HCID 46219930, compound

HRID 1924521Notes

Reaction equation

HRID 1924521 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([O:20][C:21]([F:24])([F:23])[F:22])[CH:15]=2)[N:8]=1)=O.[C:26]1([CH3:34])[CH:31]=[CH:30][C:29]([NH:32]N)=[CH:28][CH:27]=1>>[C:26]1([CH3:34])[CH:31]=[CH:30][C:29]([N:32]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[C:16]([O:20][C:21]([F:24])([F:23])[F:22])[CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)=[CH:28][CH:27]=1

Participants

3

Reactant 2

HCID 10875(4-Methylphenyl)hydrazineHCID 593701233-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

Product 1

HCID 46219930HCID 46219930, compound

Procedure

Reaction of 3-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-6) and p-tolyl-hydrazine according to example 43 gave the desired product. MS: M=413.3 (M+H)+

Sources & evidence

ORD record
ord-1c3d2816471f42d69a0e5a1c3f894a91
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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