3-((E)-3-Dimethylamino-acryloyl)-1-(3-methansulfonyl-phenyl)-1H-pyridazin-4-one → HCID 59369987, compound

HRID 1924596Notes

Reaction equation

HRID 1924596 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([S:20]([CH3:23])(=[O:22])=[O:21])[CH:15]=2)[N:8]=1)=O.[O:25]1[C:30]2[CH:31]=[CH:32][CH:33]=[C:34]([NH:35]N)[C:29]=2[O:28][CH2:27][CH2:26]1>>[O:25]1[C:30]2[CH:31]=[CH:32][CH:33]=[C:34]([N:35]3[C:5]([C:7]4[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]5[CH:19]=[CH:18][CH:17]=[C:16]([S:20]([CH3:23])(=[O:22])=[O:21])[CH:15]=5)[N:8]=4)=[CH:4][CH:3]=[N:2]3)[C:29]=2[O:28][CH2:27][CH2:26]1

Participants

3

Reactant 2

HCID 593701713-((E)-3-Dimethylamino-acryloyl)-1-(3-methansulfonyl-phenyl)-1H-pyridazin-4-oneHCID 67432127HCID 67432127, compound

Product 1

HCID 59369987HCID 59369987, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(3-methansulfonyl-phenyl)-1H-pyridazin-4-one (A-7) and (2,3-dihydro-benzo[1,4]dioxin-5-yl)-hydrazine according to the method described for example 43. MS: M=451.2 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-0b3f4b00effa47e1bb2b751d697c0605
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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