(3-Fluorophenyl)hydrazine → HCID 59370026, compound

HRID 1924599Notes

Reaction equation

HRID 1924599 reaction equation
[F:1][C:2]1([F:25])[O:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:10]([N:11]3[CH:16]=[CH:15][C:14](=[O:17])[C:13]([C:18](=O)/[CH:19]=[CH:20]/N(C)C)=[N:12]3)[C:4]=2[O:3]1.[F:26][C:27]1[CH:28]=[C:29]([NH:33][NH2:34])[CH:30]=[CH:31][CH:32]=1>>[F:1][C:2]1([F:25])[O:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:10]([N:11]3[CH:16]=[CH:15][C:14](=[O:17])[C:13]([C:18]4[N:33]([C:29]5[CH:30]=[CH:31][CH:32]=[C:27]([F:26])[CH:28]=5)[N:34]=[CH:20][CH:19]=4)=[N:12]3)[C:4]=2[O:3]1

Participants

3

Reactant 2

HCID 581026(3-Fluorophenyl)hydrazineHCID 593701341-(2,2-Difluoro-benzo[1,3]dioxol-4-yl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one

Product 1

HCID 59370026HCID 59370026, compound

Procedure

The product was obtained starting from 1-(2,2-Difluoro-benzo[1,3]dioxol-4-yl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one (A-15) and 3-fluoro-phenylhydrazine according to the method described for example 91. MS: M=413.2 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-03006fb814e14c26b151398c4c6fe7f5
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

Loading…