4-Hydrazino-2-methylpyridine → HCID 59369976, compound

HRID 1924602Notes

Reaction equation

HRID 1924602 reaction equation
[F:1][C:2]1([F:25])[O:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:10]([N:11]3[CH:16]=[CH:15][C:14](=O)[C:13]([C:18](=[O:24])/[CH:19]=[CH:20]/N(C)C)=[N:12]3)[C:4]=2[O:3]1.[NH:26]([C:28]1[CH:33]=[CH:32][N:31]=[C:30]([CH3:34])[CH:29]=1)[NH2:27]>>[F:1][C:2]1([F:25])[O:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:10]([N:11]3[CH:20]=[CH:19][C:18](=[O:24])[C:13]([C:14]4[N:26]([C:28]5[CH:33]=[CH:32][N:31]=[C:30]([CH3:34])[CH:29]=5)[N:27]=[CH:16][CH:15]=4)=[N:12]3)[C:4]=2[O:3]1

Participants

3

Reactant 2

HCID 200736634-Hydrazino-2-methylpyridineHCID 593701341-(2,2-Difluoro-benzo[1,3]dioxol-4-yl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one

Product 1

HCID 59369976HCID 59369976, compound

Procedure

The product was obtained starting from 1-(2,2-Difluoro-benzo[1,3]dioxol-4-yl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one (A-15) and 4-hydrazino-2-methylpyridine according to the method described for example 91. MS: M=410.3 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-8c1f22b39b80429fa69949306a2ecd1f
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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