4-Hydrazinobenzonitrile → HCID 59370080, compound

HRID 1924611Notes

Reaction equation

HRID 1924611 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[NH:26]([C:28]1[CH:35]=[CH:34][C:31]([C:32]#[N:33])=[CH:30][CH:29]=1)N>C(O)C>[O:13]=[C:12]1[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=[C:7]1[C:5]1[N:26]([C:28]2[CH:35]=[CH:34][C:31]([C:32]#[N:33])=[CH:30][CH:29]=2)[N:2]=[CH:3][CH:4]=1

Participants

4

Reactant 2

HCID 5837844-HydrazinobenzonitrileHCID 593700343-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

Product 1

HCID 59370080HCID 59370080, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-8) and 4-hydrazino-benzonitrile in ethanol as solvent according to the method described for example 43. MS: M=424.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-640a2bafc2c04d30afd6217e374a3491
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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