(3-Methanesulfonylphenyl)hydrazine → HCID 59370154, compound

HRID 1924613Notes

Reaction equation

HRID 1924613 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[CH3:26][S:27]([C:30]1[CH:31]=[C:32]([NH:36]N)[CH:33]=[CH:34][CH:35]=1)(=[O:29])=[O:28]>>[CH3:26][S:27]([C:30]1[CH:31]=[C:32]([N:36]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([O:20][C:21]([F:23])([F:24])[F:22])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)[CH:33]=[CH:34][CH:35]=1)(=[O:28])=[O:29]

Participants

3

Reactant 2

HCID 22034382(3-Methanesulfonylphenyl)hydrazineHCID 593700343-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

Product 1

HCID 59370154HCID 59370154, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-8) and (3-methanesulfonyl-phenyl)-hydrazine according to the method described for example 91. MS: M=477.0 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-a426940ac92d4ea6910e87e08502543f
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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