(3-Chlorophenyl)hydrazine → HCID 59370157, compound

HRID 1924616Notes

Reaction equation

HRID 1924616 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[Cl:26][C:27]1[CH:28]=[C:29]([NH:33][NH2:34])[CH:30]=[CH:31][CH:32]=1>>[Cl:26][C:27]1[CH:28]=[C:29]([N:33]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([O:20][C:21]([F:23])([F:22])[F:24])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:34]2)[CH:30]=[CH:31][CH:32]=1

Participants

3

Reactant 2

HCID 75332(3-Chlorophenyl)hydrazineHCID 593700343-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

Product 1

HCID 59370157HCID 59370157, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-8) and 3-chloro-phenylhydrazine according to the method described for example 91. MS: M=433.3 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-57bbaae2b2b745369e0c7a712bd71080
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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