(4-Fluorophenyl)hydrazine → HCID 59370102, compound
Reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([OH:20])[CH:15]=2)[N:8]=1)=O.[F:22][C:23]1[CH:28]=[CH:27][C:26]([NH:29]N)=[CH:25][CH:24]=1>>[F:22][C:23]1[CH:28]=[CH:27][C:26]([N:29]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[C:16]([OH:20])[CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)=[CH:25][CH:24]=1Participants
3
Procedure
The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(3-hydroxyphenyl)-1H-pyridazin-4-one (A-17) and 4-fluoro-phenylhydrazine according to the method described for example 43. MS: M=349.1 (M+H)+
Workup
- customThe product was obtained
Sources & evidence
- ORD record
- ord-54405d09aee045e79a3f86608a9d0140
- Source dataset
- uspto-grants-2012_05
- Patent number
- US08178538B2
Reaction notes
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