(3-Chlorophenyl)hydrazine → HCID 46219195, compound
Reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:8]=1)=O.[Cl:21][C:22]1[CH:23]=[C:24]([NH:28]N)[CH:25]=[CH:26][CH:27]=1>>[Cl:21][C:22]1[CH:23]=[C:24]([N:28]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:2]2)[CH:25]=[CH:26][CH:27]=1Participants
3
Procedure
The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-phenyl-1H-pyridazin-4-one (A-1) and 3-chloro-phenylhydrazine according to the method described for example 1. MS: M=349.2 (M+H)+
Workup
- customThe product was obtained
Sources & evidence
- ORD record
- ord-1b34cb3011bb494db9064edabdc33da9
- Source dataset
- uspto-grants-2012_05
- Patent number
- US08178538B2
Reaction notes
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