p-Hydrazinobenzenesulphonamide → HCID 59370065, compound

HRID 1924655Notes

Reaction equation

HRID 1924655 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[NH:26]([C:28]1[CH:33]=[CH:32][C:31]([S:34]([NH2:37])(=[O:36])=[O:35])=[CH:30][CH:29]=1)[NH2:27]>>[O:13]=[C:12]1[CH:11]=[CH:10][N:9]([C:14]2[CH:15]=[CH:16][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:18][CH:19]=2)[N:8]=[C:7]1[C:5]1[N:26]([C:28]2[CH:33]=[CH:32][C:31]([S:34]([NH2:37])(=[O:35])=[O:36])=[CH:30][CH:29]=2)[N:27]=[CH:3][CH:4]=1

Participants

3

Reactant 2

HCID 78105p-HydrazinobenzenesulphonamideHCID 593700343-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

Product 1

HCID 59370065HCID 59370065, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-8) and 4-hydrazino-benzenesulfonamide according to the method described for example 43. MS: M=478.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-3037480a62134d6a9b9a6947878955d6
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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