2-Chloro-4-hydrazinylpyridine → HCID 59370083, compound

HRID 1924662Notes

Reaction equation

HRID 1924662 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[NH:26]([C:28]1[CH:33]=[CH:32][N:31]=[C:30]([Cl:34])[CH:29]=1)[NH2:27]>>[Cl:34][C:30]1[CH:29]=[C:28]([N:26]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([O:20][C:21]([F:24])([F:23])[F:22])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:27]2)[CH:33]=[CH:32][N:31]=1

Participants

3

Reactant 2

HCID 211064422-Chloro-4-hydrazinylpyridineHCID 593700343-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one

Product 1

HCID 59370083HCID 59370083, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethoxy-phenyl)-1H-pyridazin-4-one (A-8) and 4-hydrazino-2-chloropyridine according to the method described for example 43. MS: M=434.0 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-4e29f61094f34da99d434793e7118886
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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