(3-Chlorophenyl)hydrazine → HCID 46220471, compound

HRID 1924675Notes

Reaction equation

HRID 1924675 reaction equation
[F:1][CH:2]([F:24])[O:3][C:4]1[CH:5]=[C:6]([N:10]2[CH:15]=[CH:14][C:13](=[O:16])[C:12]([C:17](=O)/[CH:18]=[CH:19]/[N:20](C)C)=[N:11]2)[CH:7]=[CH:8][CH:9]=1.[Cl:25][C:26]1[CH:27]=[C:28]([NH:32]N)[CH:29]=[CH:30][CH:31]=1>>[Cl:25][C:26]1[CH:27]=[C:28]([N:32]2[C:17]([C:12]3[C:13](=[O:16])[CH:14]=[CH:15][N:10]([C:6]4[CH:7]=[CH:8][CH:9]=[C:4]([O:3][CH:2]([F:24])[F:1])[CH:5]=4)[N:11]=3)=[CH:18][CH:19]=[N:20]2)[CH:29]=[CH:30][CH:31]=1

Participants

3

Reactant 2

HCID 75332(3-Chlorophenyl)hydrazineHCID 593700141-(3-Difluoromethoxy-phenyl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one

Product 1

HCID 46220471HCID 46220471, compound

Procedure

The product was obtained starting from 1-(3-Difluoromethoxy-phenyl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one (A-10) and 3-chloro-phenylhydrazine according to the method described for example 91. MS: M=415.2 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-2e0218845f76471a932ef81601492249
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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