2-Fluorophenylhydrazine hydrochloride → HCID 59370006, compound

HRID 1924677Notes

Reaction equation

HRID 1924677 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:15]=[C:16]([CH:22]=[CH:23][CH:24]=2)[C:17]([N:19]([CH3:21])[CH3:20])=[O:18])[N:8]=1)=O.[F:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[NH:33]N>>[F:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[N:33]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:15]=[C:16]([CH:22]=[CH:23][CH:24]=3)[C:17]([N:19]([CH3:21])[CH3:20])=[O:18])[N:8]=2)=[CH:4][CH:3]=[N:2]1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370129HCID 59370129, compound

Product 1

HCID 59370006HCID 59370006, compound

Procedure

The product was obtained starting from 3-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N,N-dimethyl-benzamide (A-20) and 2-fluoro-phenylhydrazine according to the method described for example 91. MS: M=404.3 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-aa9ba074b3c247d5a6277e26db255416
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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