(3-Chlorophenyl)hydrazine → HCID 59369947, compound

HRID 1924678Notes

Reaction equation

HRID 1924678 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:15]=[C:16]([CH:22]=[CH:23][CH:24]=2)[C:17]([N:19]([CH3:21])[CH3:20])=[O:18])[N:8]=1)=O.[Cl:26][C:27]1[CH:28]=[C:29]([NH:33]N)[CH:30]=[CH:31][CH:32]=1>>[Cl:26][C:27]1[CH:28]=[C:29]([N:33]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:15]=[C:16]([CH:22]=[CH:23][CH:24]=4)[C:17]([N:19]([CH3:21])[CH3:20])=[O:18])[N:8]=3)=[CH:4][CH:3]=[N:2]2)[CH:30]=[CH:31][CH:32]=1

Participants

3

Reactant 2

HCID 75332(3-Chlorophenyl)hydrazineHCID 59370129HCID 59370129, compound

Product 1

HCID 59369947HCID 59369947, compound

Procedure

The product was obtained starting from 3-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N,N-dimethyl-benzamide (A-20) and 3-chloro-phenylhydrazine according to the method described for example 91. MS: M=420.2 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-e6a25855659e43d280208edabb6a6494
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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