(3-Chlorophenyl)hydrazine → HCID 59370077, compound

HRID 1924682Notes

Reaction equation

HRID 1924682 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][CH:15]=2)[N:8]=1)=O.[Cl:25][C:26]1[CH:27]=[C:28]([NH:32][NH2:33])[CH:29]=[CH:30][CH:31]=1>>[Cl:25][C:26]1[CH:27]=[C:28]([N:32]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([C:20]([F:22])([F:21])[F:23])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:33]2)[CH:29]=[CH:30][CH:31]=1

Participants

3

Reactant 2

HCID 75332(3-Chlorophenyl)hydrazineHCID 5704110HCID 5704110, compound

Product 1

HCID 59370077HCID 59370077, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethyl-phenyl)-1H-pyridazin-4-one (A-22) and 3-chloro-phenylhydrazine according to the method described for example 1. MS: M=417.2 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-ec078fc56a2b46159956a1764093835d
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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