o-Tolylhydrazine → HCID 59369998, compound

HRID 1924685Notes

Reaction equation

CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][CH:15]=2)[N:8]=1)=O.[C:25]1([CH3:33])[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[NH:31][NH2:32]>>[C:25]1([CH3:33])[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[N:31]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:19]=[CH:18][C:17]([C:20]([F:22])([F:21])[F:23])=[CH:16][CH:15]=3)[N:8]=2)=[CH:4][CH:3]=[N:32]1

Participants

Reactant 2

HCID 68256o-Tolylhydrazine

HCID 5704110HCID 5704110, compound

Product 1

HCID 59369998HCID 59369998, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethyl-phenyl)-1H-pyridazin-4-one (A-22) and o-tolylhydrazine according to the method described for example 1. MS: M=397.1 (M+H)+

Workup

customThe product was obtained

Sources & evidence

ORD record: ord-049ecf2cde574974a2210836355504d8
Source dataset: uspto-grants-2012_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08178538B2

Reaction notes

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