2-Fluorophenylhydrazine hydrochloride → HCID 59370120, compound

HRID 1924686Notes

Reaction equation

HRID 1924686 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[CH:13]=[CH:12][C:11](=[O:14])[C:10]([C:15](=O)/[CH:16]=[CH:17]/[N:18](C)C)=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[F:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][C:24]=1[NH:29]N>>[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[CH:13]=[CH:12][C:11](=[O:14])[C:10]([C:15]3[N:29]([C:24]4[CH:25]=[CH:26][CH:27]=[CH:28][C:23]=4[F:22])[N:18]=[CH:17][CH:16]=3)=[N:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370045HCID 59370045, compound

Product 1

HCID 59370120HCID 59370120, compound

Procedure

The product was obtained starting from 1-(3-Chloro-phenyl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one (A-23) and 2-fluoro-phenylhydrazine according to the method described for example 1. MS: M=367.0 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-74ca3af2a17b4e19b1f3868025f8fc6d
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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