(3-Chlorophenyl)hydrazine → HCID 59369946, compound

HRID 1924687Notes

Reaction equation

HRID 1924687 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[CH:13]=[CH:12][C:11](=[O:14])[C:10]([C:15](=O)/[CH:16]=[CH:17]/[N:18](C)C)=[N:9]2)[CH:5]=[CH:6][CH:7]=1.[Cl:22][C:23]1[CH:24]=[C:25]([NH:29]N)[CH:26]=[CH:27][CH:28]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([N:8]2[CH:13]=[CH:12][C:11](=[O:14])[C:10]([C:15]3[N:29]([C:25]4[CH:26]=[CH:27][CH:28]=[C:23]([Cl:22])[CH:24]=4)[N:18]=[CH:17][CH:16]=3)=[N:9]2)[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 75332(3-Chlorophenyl)hydrazineHCID 59370045HCID 59370045, compound

Product 1

HCID 59369946HCID 59369946, compound

Procedure

The product was obtained starting from 1-(3-Chloro-phenyl)-3-((E)-3-dimethylamino-acryloyl)-1H-pyridazin-4-one (A-23) and 3-chloro-phenylhydrazine according to the method described for example 1. MS: M=383.0 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-67c3f5114807436b801ecca2b2b21fa2
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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