2-Fluorophenylhydrazine hydrochloride → HCID 59370179, compound

HRID 1924701Notes

Reaction equation

HRID 1924701 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([CH2:20][N:21]([CH3:23])[CH3:22])=[CH:16][CH:15]=2)[N:8]=1)=O.[F:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[NH:32]N>>[CH3:22][N:21]([CH2:20][C:17]1[CH:18]=[CH:19][C:14]([N:9]2[CH:10]=[CH:11][C:12](=[O:13])[C:7]([C:5]3[N:32]([C:27]4[CH:28]=[CH:29][CH:30]=[CH:31][C:26]=4[F:25])[N:2]=[CH:3][CH:4]=3)=[N:8]2)=[CH:15][CH:16]=1)[CH3:23]

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370089HCID 59370089, compound

Product 1

HCID 59370179HCID 59370179, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-dimethylaminomethyl-phenyl)-1H-pyridazin-4-one (A-28) and 2-fluoro-phenylhydrazine according to the method described for example 91. MS: M=390.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-87522750f8a14589b31c4471a3ca8a18
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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