2-Fluorophenylhydrazine hydrochloride → HCID 59370056, compound

HRID 1924707Notes

Reaction equation

HRID 1924707 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([S:20]([NH:23][CH3:24])(=[O:22])=[O:21])=[CH:16][CH:15]=2)[N:8]=1)=O.[F:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[NH:33][NH2:34]>>[F:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=1[N:33]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:19]=[CH:18][C:17]([S:20]([NH:23][CH3:24])(=[O:22])=[O:21])=[CH:16][CH:15]=3)[N:8]=2)=[CH:4][CH:3]=[N:34]1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370052HCID 59370052, compound

Product 1

HCID 59370056HCID 59370056, compound

Procedure

The product was obtained starting from 4-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N-methyl-benzenesulfonamide (A-30) and 2-fluoro-phenylhydrazine according to the method described for example 91. MS: M=426.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-63f16e5563ab4f1fae675ca9c82ef787
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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