7-Chloro-4-hydrazinylquinoline → HCID 59370145, compound

HRID 1924720Notes

Reaction equation

HRID 1924720 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:15]=[C:16]([S:20]([N:23]([CH2:26][CH3:27])[CH2:24][CH3:25])(=[O:22])=[O:21])[CH:17]=[CH:18][CH:19]=2)[N:8]=1)=O.[Cl:29][C:30]1[CH:39]=[C:38]2[C:33]([C:34]([NH:40][NH2:41])=[CH:35][CH:36]=[N:37]2)=[CH:32][CH:31]=1>>[Cl:29][C:30]1[CH:39]=[C:38]2[C:33]([C:34]([N:40]3[C:5]([C:7]4[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]5[CH:15]=[C:16]([S:20]([N:23]([CH2:24][CH3:25])[CH2:26][CH3:27])(=[O:22])=[O:21])[CH:17]=[CH:18][CH:19]=5)[N:8]=4)=[CH:4][CH:3]=[N:41]3)=[CH:35][CH:36]=[N:37]2)=[CH:32][CH:31]=1

Participants

3

Reactant 2

HCID 321097-Chloro-4-hydrazinylquinolineHCID 593700613-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N,N-diethyl-benzenesulfonamide

Product 1

HCID 59370145HCID 59370145, compound

Procedure

The product was obtained starting from 3-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N,N-diethyl-benzenesulfonamide (A-21) and (7-chloro-quinolin-4-yl)-hydrazine according to the method described for example 91. MS: M=533.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-9060f6ecb2744d829155ab559d389d9c
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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