2-Fluorophenylhydrazine hydrochloride → HCID 59370040, compound

HRID 1924723Notes

Reaction equation

HRID 1924723 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][CH2:21][C:22]([F:25])([F:24])[F:23])=[CH:16][CH:15]=2)[N:8]=1)=O.[F:27][C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][C:29]=1[NH:34][NH2:35]>>[F:27][C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][C:29]=1[N:34]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:19]=[CH:18][C:17]([O:20][CH2:21][C:22]([F:24])([F:25])[F:23])=[CH:16][CH:15]=3)[N:8]=2)=[CH:4][CH:3]=[N:35]1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370013HCID 59370013, compound

Product 1

HCID 59370040HCID 59370040, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-[4-(2,2,2-trifluoro-ethoxy)-phenyl]-1H-pyridazin-4-one (A-32) and 2-fluoro-phenylhydrazine according to the method described for example 43. MS: M=431.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-8a216ee83f694ab18b99f1ea84be01e4
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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