(3-Chlorophenyl)hydrazine → HCID 59370060, compound

HRID 1924725Notes

Reaction equation

HRID 1924725 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([O:20][CH2:21][C:22]([F:25])([F:24])[F:23])=[CH:16][CH:15]=2)[N:8]=1)=O.[Cl:27][C:28]1[CH:29]=[C:30]([NH:34][NH2:35])[CH:31]=[CH:32][CH:33]=1>>[Cl:27][C:28]1[CH:29]=[C:30]([N:34]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([O:20][CH2:21][C:22]([F:24])([F:23])[F:25])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:35]2)[CH:31]=[CH:32][CH:33]=1

Participants

3

Reactant 2

HCID 75332(3-Chlorophenyl)hydrazineHCID 59370013HCID 59370013, compound

Product 1

HCID 59370060HCID 59370060, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-[4-(2,2,2-trifluoro-ethoxy)-phenyl]-1H-pyridazin-4-one (A-32) and 3-chloro-phenylhydrazine according to the method described for example 43. MS: M=447.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-f6d72131818c48fba4cab079dcff8ec5
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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