(3-Fluorophenyl)hydrazine → HCID 59369961, compound

HRID 1924740Notes

Reaction equation

HRID 1924740 reaction equation
CN(C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][C:17]([S:20]([NH:23][CH3:24])(=[O:22])=[O:21])=[CH:16][CH:15]=2)[N:8]=1)=O.[F:26][C:27]1[CH:28]=[C:29]([NH:33][NH2:34])[CH:30]=[CH:31][CH:32]=1>>[F:26][C:27]1[CH:28]=[C:29]([N:33]2[C:5]([C:7]3[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]4[CH:19]=[CH:18][C:17]([S:20]([NH:23][CH3:24])(=[O:22])=[O:21])=[CH:16][CH:15]=4)[N:8]=3)=[CH:4][CH:3]=[N:34]2)[CH:30]=[CH:31][CH:32]=1

Participants

3

Reactant 2

HCID 581026(3-Fluorophenyl)hydrazineHCID 59370052HCID 59370052, compound

Product 1

HCID 59369961HCID 59369961, compound

Procedure

The product was obtained starting from 4-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N-methyl-benzenesulfonamide (A-30) and 3-fluoro-phenylhydrazine according to the method described for example 91. MS: M=426.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-bdf76ad709404265b203a7f92790ef68
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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