(2,3-Dihydro-benzo[1,4]dioxin-6-yl)-hydrazine → HCID 59370164, compound

HRID 1924745Notes

Reaction equation

HRID 1924745 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([OH:20])[CH:15]=2)[N:8]=1)=O.[O:22]1[C:27]2[CH:28]=[CH:29][C:30]([NH:32]N)=[CH:31][C:26]=2[O:25][CH2:24][CH2:23]1>>[O:22]1[C:27]2[CH:28]=[CH:29][C:30]([N:32]3[C:5]([C:7]4[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]5[CH:19]=[CH:18][CH:17]=[C:16]([OH:20])[CH:15]=5)[N:8]=4)=[CH:4][CH:3]=[N:2]3)=[CH:31][C:26]=2[O:25][CH2:24][CH2:23]1

Participants

3

Reactant 2

HCID 5164485(2,3-Dihydro-benzo[1,4]dioxin-6-yl)-hydrazineHCID 59370010HCID 59370010, compound

Product 1

HCID 59370164HCID 59370164, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(3-hydroxyphenyl)-1H-pyridazin-4-one (A-17) and (2,3-dihydro-benzo[1,4]dioxin-6-yl)-hydrazine according to the method described for example 91. MS: M=389.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-bed9e52fcf404a37922098bd99fbf788
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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