2-Fluorophenylhydrazine hydrochloride → HCID 46218709, compound

HRID 1924758Notes

Reaction equation

HRID 1924758 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:15]=[C:16]([NH:20][C:21](=[O:23])[CH3:22])[CH:17]=[CH:18][CH:19]=2)[N:8]=1)=O.[F:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[NH:32]N>>[F:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[N:32]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:15]=[C:16]([NH:20][C:21](=[O:23])[CH3:22])[CH:17]=[CH:18][CH:19]=3)[N:8]=2)=[CH:4][CH:3]=[N:2]1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370112HCID 59370112, compound

Product 1

HCID 46218709HCID 46218709, compound

Procedure

The product was obtained starting from N-{3-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-phenyl}-acetamide (A-34) and 2-fluoro-phenylhydrazine according to the method described for example 1. MS: M=390.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-53ecae4353f74534b09a0d95f1c9eec6
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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