2-Fluorophenylhydrazine hydrochloride → HCID 46218710, compound

HRID 1924759Notes

Reaction equation

HRID 1924759 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=2)[C:17]([NH:19][CH3:20])=[O:18])[N:8]=1)=O.[F:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[NH:32]N>>[F:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[N:32]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=3)[C:17]([NH:19][CH3:20])=[O:18])[N:8]=2)=[CH:4][CH:3]=[N:2]1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370022HCID 59370022, compound

Product 1

HCID 46218710HCID 46218710, compound

Procedure

The product was obtained starting from 3-[3-((E)-3-Dimethylamino-acryloyl)-4-oxo-4H-pyridazin-1-yl]-N-methyl-benzamide (A-35) and 2-fluoro-phenylhydrazine according to the method described for example 1. MS: M=390.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-b9453ba4b13b44b18f49d4ea8ae3907f
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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