2-Fluorophenylhydrazine hydrochloride → HCID 59370165, compound

HRID 1924762Notes

Reaction equation

HRID 1924762 reaction equation
C[N:2](C)/[CH:3]=[CH:4]/[C:5]([C:7]1[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]2[CH:19]=[CH:18][CH:17]=[C:16]([CH:20]([OH:22])[CH3:21])[CH:15]=2)[N:8]=1)=O.[F:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[NH:31]N>>[F:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[N:31]1[C:5]([C:7]2[C:12](=[O:13])[CH:11]=[CH:10][N:9]([C:14]3[CH:19]=[CH:18][CH:17]=[C:16]([CH:20]([OH:22])[CH3:21])[CH:15]=3)[N:8]=2)=[CH:4][CH:3]=[N:2]1

Participants

3

Reactant 2

HCID 4238442-Fluorophenylhydrazine hydrochlorideHCID 59370041HCID 59370041, compound

Product 1

HCID 59370165HCID 59370165, compound

Procedure

The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-[3-(1-hydroxy-ethyl)-phenyl]-1H-pyridazin-4-one (A-36) and 2-fluoro-phenylhydrazine according to the method described for example 1. MS: M=377.1 (M+H)+

Workup

  1. customThe product was obtained

Sources & evidence

ORD record
ord-be2bf70429ef4a4994d552642a176fbc
Source dataset
uspto-grants-2012_05
Patent number
US08178538B2

Reaction notes

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