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HRID1924769

反应详情

EQUATION

反应方程式

HRID 1924769 的结构方程式

REACTANTS

反应物

2
结构：Cc1n[nH]c(C)c1B1OC(C)(C)C(C)(C)O1
HCID16217713

3,5-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole

C11H19BN2O2

结构：CC(C)(O)c1ccc(C(=O)Nc2nc3ccc(Br)nc3s2)cc1
HCID58015365

未命名化合物

PRODUCTS

生成物

1
结构：Cc1n[nH]c(C)c1-c1ccc2nc(NC(=O)c3ccc(C(C)(C)O)cc3)sc2n1
HCID44549075

未命名化合物

收率 25%

PROCEDURE

实验过程

The titled compound (yield=25%, white solid) was prepared using a procedure analogous to that described in connection with 9 (Example 9) except 1D (Example 1) and 3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole were used as starting materials. 1H NMR (400 MHz, DMSO-d6) δ ppm 1.46 (s, 6H) 2.40 (s, 6H) 7.54 (d, J=8.34 Hz, 1H) 7.66 (d, J=8.34 Hz, 2H) 8.04-8.19 (m, 3H) 12.89 (br. s., 1H); ESI-MS: m/z 408.0 (M+H)+.