HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24823730, compound → 7-Hydroxy-quinoline-4-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24823730 | HCID 24823730 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Boron tribromide | HCID 25134 | — |
| Product | 7-Hydroxy-quinoline-4-carboxylic acid | HCID 135783305 | — |
Reaction Steps
To a cooled (0° C.) solution of methyl 7-methoxyquinoline-4-carboxylate (378 mg, 1.74 mmol) in CH2Cl2, BBr3 (9 mL, excess) was added and the reaction mixture stirred and warmed to RT. After 4 days, the mixture was poured into ice and the yellow solid collected as the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178557B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-ddc3ff49b109404f9682006e22d2c5c3 |
| Source note | uspto-grants-2012_05 |