HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Methoxy-3-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Methoxy-3-nitrobenzoic acid | HCID 66640 | — |
| Product | 4-Methoxy-3-nitrobenzoyl chloride | HCID 12375463 | — |
Reaction Steps
4-methoxy-3-nitrobenzoic acid (10.0 g, 0.051 mol), and thionyl chloride (25 g, 0.212 mol), were refluxed together for 24 h. The reaction mixture was cooled to RT and concentrated to dryness. The off-white solid was carried onto the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178557B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-153dd7436cdd4bf28126e895d90e9318 |
| Source note | uspto-grants-2012_05 |