HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1925493Generated: October 29, 2026
3-Hydroxybenzaldehyde → HCID 6365568, compound
https://huagongshe.com/reaction/1925493
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Hydroxybenzaldehyde | HCID 101 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 6365568 | HCID 6365568 | 82.6% |
Reaction Steps
To a solution of 3-hydroxybenzaldehyde (20 g, 0.16 mol) in acetic acid (40 mL) was added nitro ethane (32 mL, 0.45 mol) and ammonium acetate (8 g, 0.1 mol). The resulting mixture was stirred at 80° C. for 6 hours. The reaction mixture was poured into a solution of 400 mL of water and the precipitate was collected by filtration to obtain the title compound as a solid (23.68 g, 81%). MS (M+): 180.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08178679B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-1dcb62f6bd2d405f811042ea5b555ed4 |
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| Source note | uspto-grants-2012_05 |
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