HCID 67520692, compound → HCID 59180376, compound

Participants

Reaction Steps

A suspension of 25 (206.0 mg; 0.47 mmol) and palladium on carbon (103.0 mg; 0.91 mmol) in ethanol (2.3 mL) was evacuated and filled with hydrogen gas (3×) and then stirred at room temperature under hydrogen overnight. Additional palladium on carbon (103.0 mg) was added and stirring was continued at room temperature for 16 hours. The reaction mixture filtered through celite and the filtrate concentrated under reduced pressure to afford the title compound as a clear oil (143 mg).

Provenance & Evidence