HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 19683023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Methyl 3-amino-2-thiophenecarboxylate | HCID 89652 | — |
| Reactant | 4-(Propan-2-yl)benzene-1-sulfonyl chloride | HCID 2734882 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19683023 | HCID 19683023 | 64.5% |
Reaction Steps
Synthesized as described for 52 using commercially available 4-iso-propylbenzenesulfonyl chloride (1.0 g; 4.57 mmol), methyl 3-aminothiophene-2-carboxylate (0.72 g; 4.57 mmol), pyridine (0.55 mL; 6.86 mmol), and anhydrous dichloromethane (3 mL). This afforded the title compound as a white solid (1.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08178699B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-6a6fe1d157e349dd8f620cd38e01301f |
| Source note | uspto-grants-2012_05 |