2,3-Difluoroaniline → HCID 178505565, compound

HRID 1926412Notes

Reaction equation

HRID 1926412 reaction equation
F[C:2]1[C:8]([F:9])=[CH:7][CH:6]=[CH:5][C:3]=1[NH2:4].ClC1C=CC2[S:18][C:17]([SH:19])=NC=2C=1>>[F:9][C:8]1[C:2]2[S:18][C:17]([SH:19])=[N:4][C:3]=2[CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 782782,3-DifluoroanilineHCID 178527796HCID 178527796, compound

Product 1

HCID 178505565HCID 178505565, compound

Conditions

Temperature
90 °C

Procedure

The title compound was prepared from 2,3-difluoroaniline as described for 5-chloro-2-mercaptobenzothiazole except that in the first step the reaction mixture was heated to 90° C. for 4 h.

Sources & evidence

ORD record
ord-599bde9334aa419e8e7793d8128c3282
Source dataset
uspto-grants-2012_05
Patent number
US08178668B2

Reaction notes

Loading…