Nickel perchlorate hexahydrate → HCID 86619911, compound

HRID 1926461Notes

Reaction equation

HRID 1926461 reaction equation
O.O.O.O.O.O.Cl([O-])(=O)(=O)=O.[Ni+2:12].Cl([O-])(=O)(=O)=O.O.[CH2:19]([P:23]([CH2:26][CH:27]([CH3:29])[CH3:28])(=[S:25])[S-:24])[CH:20]([CH3:22])[CH3:21].[Na+]>O>[CH2:19]([P:23]([CH2:26][CH:27]([CH3:29])[CH3:28])(=[S:24])[S-:25])[CH:20]([CH3:22])[CH3:21].[CH2:19]([P:23]([CH2:26][CH:27]([CH3:29])[CH3:28])(=[S:24])[S-:25])[CH:20]([CH3:22])[CH3:21].[Ni+2:12]

Participants

4

Reactant 2

HCID 15769463Nickel perchlorate hexahydrateHCID 86619912HCID 86619912, compound

Product 1

HCID 86619911HCID 86619911, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

0.55 g Nickel(II) perchlorate hexahydrate was dissolved in 0.5 ml of water. 0.60 g of a 50% sodium di(isobutyl)dithiophosphinate water solution and another 2.5 ml water were added. A dark purple precipitate formed immediately. The precipitate was collected by vacuum filtration and washed with three 5 ml portions of water. The precipitate was dried at 50 C in a vacuum oven.

Workup

  1. customA dark purple precipitate formed immediately
  2. filtrationThe precipitate was collected by vacuum filtration
  3. washwashed with three 5 ml portions of water
  4. customThe precipitate was dried at 50 C in a vacuum oven

Sources & evidence

ORD record
ord-dea2dcfc05c74abd8be8761e95769c8a
Source dataset
uspto-grants-2012_05
Patent number
US08182718B2

Reaction notes

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