HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylolpropionic acid → HCID 86619916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylolpropionic acid | HCID 78501 | — |
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86619916 | HCID 86619916 | — |
Reaction Steps
To a flask were added 3.0 g 2,2-bis(hydroxymethyl)propionic acid, 9.5 g of a 55-60% solution of tetrabutylammonium hydroxide in water and 40 ml 2-propanol. After heating to 50 C under nitrogen for 1 hour, the solvent was removed and another 40 ml of 2-propanol were added and removed by distillation under reduced pressure. After drying, a pale yellow oil was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08182718B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-7c06ee8f4e174bbca15a6a8bd1f16d3a |
| Source note | uspto-grants-2012_05 |