HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20097836, compound → HCID 59627195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20097836 | HCID 20097836 | — |
| Reactant | HCID 59627173 | HCID 59627173 | — |
| Reactant | HCID 59627186 | HCID 59627186 | — |
| Product | HCID 59627195 | HCID 59627195 | 50% |
Reaction Steps
1-(Bromomethyl)-5-chloro-3-methyl-2-nitrobenzene (38) Following the procedure for the preparation of 1-(bromomethyl)-2-nitro-3-(trifluoromethyl)benzene (17) in Example 3, reaction of 5-chloro-1,3-dimethyl-2-nitrobenzene (37) provided the title compound as a solid (50%). 1H NMR (400 MHz, CDCl3) δ 2.36 (m, 3H), 4.43 (s, 2H), 7.28 (m, 1H), 7.37 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183238B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-856bd0e7fd184aada3954fbc24eb3047 |
| Source note | uspto-grants-2012_05 |