HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59627090, compound → HCID 59627097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59627090 | HCID 59627090 | — |
| Reactant | HCID 59627093 | HCID 59627093 | — |
| Product | HCID 59627097 | HCID 59627097 | — |
Reaction Steps
Methyl N-(tert-butoxycarbonyl)-2-nitro-5-(phenylsulfonyl)-L-phenylalaninate (70) Compound 70 was prepared from 2-bromo-1-nitro-4-(phenylsulfonyl)benzene (69) according to the general procedure for the synthesis of methyl N-(tert-butoxycarbonyl)-3-(2-nitro-5-phenoxypyridin-3-yl)-L-alaninate (65) in Example 66. The product was obtained as an off-white foam (250 mg, 37%). LCMS m/z 463.1 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08183238B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-e07d6937b7f84ef6bb99876531bb2217 |
| Source note | uspto-grants-2012_05 |