HRID1927053

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID7666

Phenethyl bromide

C8H9Br

反应SMILES：OC(c1cccs1)(c1cccs1)C12CCN(CC1)CC2

HCID68865599

1-Azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol

C16H19NOS2

PRODUCTS

产物

反应SMILES：OC(c1cccs1)(c1cccs1)C12CC[N+](CCc3ccccc3)(CC1)CC2.[Br-]

HCID11641678

未命名化合物

收率 3,792.8%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

Following the general procedure outlined in Example 4, 1-azabicyclo[2.2.2]oct-4-yl(di-2-thienyl)methanol (0.0658 g, 0.215 mmol) and (2-bromoethyl)benzene (0.050 mL, 0.366 mmol) in 1MeOH/1 CHCl3 (4.0 mL) were reacted to give the desired product (0.051 4 g, 48.9%). EI-MS m/z 410 (M+) Rt (1.83 min).

WORKUP

后处理

customwere reacted