HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1927446Generated: November 1, 2026
4-Fluorobenzene-1,2-diamine → HCID 25004451, compound
https://huagongshe.com/reaction/1927446
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Fluorobenzene-1,2-diamine | HCID 164584 | — |
| Reactant | (E)-3-[3-methoxy-4-(4-methylimidazol-1-yl)phenyl]acrylic acid | HCID 59528030 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 25004451 | HCID 25004451 | — |
Reaction Steps
(E)-3-[3-Methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-acrylic acid (100 mg, 0.39 mmol) and 4-fluorobenzene-1,2-diamine (49 mg, 0.39 mmol) were placed in a 4-mL vial. Ethylene glycol (1 ml) was added and the reaction mixture heated to 100° C. for 16 h and then to 165° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08183276B2 |
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| Source dataset | uspto-grants-2012_05 |
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| ORD ID | ord-5d76f4a4bb8d4bedae0fb1ca74bd3372 |
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| Source note | uspto-grants-2012_05 |
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